| Metrology area, Sub-field | Chemistry and Biology, Organics |
| Description | Measurement of PAHs in protein matrix |
| Time of measurements | 2022 - 2024 |
| Status | Approved |
| Final Reports of the comparisons | |
| References | |
| Measurand | Mass fraction of benz(a)anthracene (BaA) in a high protein matrix, Mass fraction of benzo(a)pyrene (BaP) in a high protein matrix, Mass fraction of benzo(b)fluoranthene (BbF) in a high protein matrix, mass fraction of chrysene (Chr) in a high protein matrix. 0.1 µg/kg to 50 µg/kg |
| Parameters | see protocol |
| Transfer device | Sample in form of a powder |
| Comparison type | Supplementary Comparison |
| Consultative Committee | CCQM (Consultative Committee for Amount of Substance) |
| Conducted by | EURAMET (European Association of National Metrology Institutes) |
| Comments | Polycyclic aromatic hydrocarbons (PAH) are a class of chemicals, consisting of hydrocarbons with at least two connected aromatic ring systems. They may be produced during the processing of foodstuffs, such as smoking. They may, however, also find their way into foodstuffs unintentionally, e.g. from mineral oils. Because they may have negative effects on health – they are associated with cancer and other diseases – threshold values have been set for PAHs. Accurate analyses regarding these chemicals are therefore called for. There were other comparisons previously conducted for the determination of PAHs. CCQM conducted key comparisons with final reports published in 2018 (CCQM-K95.1: Polycyclic Aromatic Hydrocarbons (PAHs) in Tea) and 2020 (CCQM-K146: Benzo[a]pyrene in Olive Oil). So far, however, no comparison of PAHs in a protein-rich matrix has been carried out. In this comparison the target PAHs are benz(a)anthracene (BaA), benzo(a)pyrene (BaP), benzo(b)fluoranthene (BbF), and chrysene (Chr) in a protein-rich matrix. Successful participation in this supplementary comparison will demonstrate the measurement capabilities in determining mass fractions of low polarity organic compounds with molecular masses of about 150 - 500 g/mol in the mass fraction range from 0.1 µg/kg to 100 µg/kg (as received) in a protein-rich matrix. |
| Pilot institute |
METAS
Federal Institute of Metrology Switzerland |
| Contact person | Gisela Umbricht +41583870581 |
| Pilot laboratory | |
|---|---|
| METAS |
Federal Institute of Metrology, Switzerland, EURAMET |
| BVL |
Bundesamt für Verbraucherschutz und Lebensmittelsicherheit, Germany, EURAMET |
| INRIM |
Istituto Nazionale di Ricerca Metrologica, Italy, EURAMET |
| IW |
Institut za vode d.o.o. Bijeljina, Bosnia and Herzegovina, EURAMET |
| MIRS/ZRS Koper/LAB-IZO |
MIRS/Science and Research Centre Koper/ Laboratory of the Institute for Oliveculture, Slovenia, EURAMET |
| UME |
TÜBITAK Ulusal Metroloji Enstitüsü, Türkiye, EURAMET |
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