MEASURAND   Mass fraction of Zinc in bovine liver

NOMINAL VALUE  50 mg/kg to 500 mg/kg

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Mass fraction of Zinc in bovine liver
Di
Participating institutes

MEASURAND    Mass fraction of Nickel in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Mass fraction of Nickel in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Phosphorus in bovine liver

NOMINAL VALUE  5 mg/g to 50 mg/g

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/g.

Mass fraction of Phosphorus in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Sulfur in bovine liver

NOMINAL VALUE  1 mg/g to 30 mg/g

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/g.

Mass fraction of Sulfur in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Manganese in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Mass fraction of Manganese in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Molybdenum in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Mass fraction of Molybdenum in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Chromium in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

Mass fraction of Chromium in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Strontium in bovine liver

NOMINAL VALUE  50 µg/kg to 500 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

Mass fraction of Strontium in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Lead in bovine liver

NOMINAL VALUE  10 µg/kg to 300 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

Mass fraction of Lead in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Cobalt in bovine liver

NOMINAL VALUE  10 µg/kg to 300 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

Mass fraction of Cobalt in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Arsenic in bovine liver

NOMINAL VALUE  1 µg/kg to 100 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

Mass fraction of Arsenic in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Mercury in bovine liver

NOMINAL VALUE  1 µg/kg to 100 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

Mass fraction of Mercury in bovine liver
Di
Participating institutes

MEASURAND   Mass fraction of Zinc in bovine liver

NOMINAL VALUE  50 mg/kg to 500 mg/kg

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
INRAP -26.5 19.1
VNIIM -20 18
LATU -3 12
INACAL -3.1 18
GL -2.6 16
NMIA -2.1 9
NIM -1.7 11
KRISS -1.7 14
LGC -1.7 8
NMISA -1.7 12
MIRS/IJS/F-2,O-2 -1 28
NIST 0.0 4.7
UME 1 8
HSA 3 14
PTB 3.2 4.2
RISE 4.3 6.8
MIKES-SYKE 4.7 23.1
INM (CO) 5 13.2
NRC 6 10
NIMT 6 26.4
NMIJ 6 6.5
KEBS 18 33
INRIM 35.5 20.2
Participating institutes
CCQM-K145

MEASURAND    Mass fraction of Nickel in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
VNIIM -1.88 0.059
NMISA -1.12 0.090
NIMT -0.37 0.13
MIRS/IJS/F-2,O-2 -0.09 0.23
INM (CO) -0.08 0.14
GL -0.08 0.19
LNE -0.064 0.16
NIST -0.038 0.064
KRISS -0.029 0.082
INACAL -0.01 0.13
NMIA -0.002 0.11
NIM 0.000 0.068
NMIJ 0.03 0.06
RISE 0.033 0.12
NRC 0.05 0.11
PTB 0.055 0.086
LATU 0.06 0.13
LGC 0.109 0.097
UME 0.13 0.08
HSA 0.16 0.2
KEBS 2.61 1.9
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Phosphorus in bovine liver

NOMINAL VALUE  5 mg/g to 50 mg/g

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/g.

LABi Di Uneg,i Upos,i
mg/g
mg/g
mg/g
VNIIM -0.75 0.53
NMISA -0.19 0.27
NMIJ -0.14 0.25
NIM -0.13 0.31
LATU 0.00 0.31
UME 0.15 0.27
NRC 0.30 0.63
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Sulfur in bovine liver

NOMINAL VALUE  1 mg/g to 30 mg/g

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/g.

LABi Di Uneg,i Upos,i
mg/g
mg/g
mg/g
VNIIM -0.65 0.46
NIM -0.08 0.23
HSA -0.05 0.38
NRC 0.14 0.33
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Manganese in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
VNIIM -0.66 0.36
LNE -0.27 0.54
MIRS/IJS/F-2,O-2 -0.18 0.34
EXHM/GCSL-EIM -0.059 0.49
NIMT -0.04 0.27
INRAP -0.01 0.52
NIM 0.005 0.13
KRISS 0.005 0.23
INACAL 0.02 0.21
LATU 0.04 0.25
NMIJ 0.17 0.13
NMISA 0.95 0.28
INRIM 0.96 0.36
KEBS 0.97 1.3
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Molybdenum in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
VNIIM -0.21 0.1
INRAP -0.19 0.13
LNE -0.14 0.12
NIMT -0.058 0.04
NMISA -0.016 0.04
KRISS -0.009 0.10
HSA -0.002 0.04
NMIA 0.002 0.03
MIRS/IJS/F-2,O-2 0.002 0.14
INM (CO) 0.003 0.05
NIM 0.011 0.03
KEBS 0.36 0.22
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Chromium in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in mg/kg.

LABi Di Uneg,i Upos,i
mg/kg
mg/kg
mg/kg
VNIIM -4.04 0.10
NMISA -2.56 0.17
NIMT -0.94 0.25
LNE -0.25 0.32
KRISS -0.196 0.13
NMIA -0.09 0.16
NIM -0.080 0.14
NMIJ -0.01 0.12
LATU 0.00 0.28
RISE 0.01 0.19
HSA 0.06 0.22
UME 0.09 0.2
MIRS/IJS/F-2,O-2 0.17 0.30
INRIM 0.51 0.32
KEBS 0.83 0.73
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Strontium in bovine liver

NOMINAL VALUE  50 µg/kg to 500 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

LABi Di Uneg,i Upos,i
µg/kg
µg/kg
µg/kg
VNIIM -2 19
NIM -0.04 12
NIMT -0.04 19
LATU 0.2 11
NRC 2 19
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Lead in bovine liver

NOMINAL VALUE  10 µg/kg to 300 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

LABi Di Uneg,i Upos,i
µg/kg
µg/kg
µg/kg
VNIIM -2.9 8
NIMT -3 6
LATU -2.4 6
INM (CO) -1.2 8.8
LNE -0.8 5.1
LGC -0.8 2.7
MIKES-SYKE -0.6 10
NIM 0.65 2.6
KRISS 0.9 5.7
UME 0.9 2.9
HSA 1.2 5.3
NRC 2 10
PTB 3.2 5.3
NMISA 5.6 4.8
KEBS 14.8 52
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Cobalt in bovine liver

NOMINAL VALUE  10 µg/kg to 300 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

LABi Di Uneg,i Upos,i
µg/kg
µg/kg
µg/kg
VNIIM -27.5 7.6
NIMT -5 12
LATU -0.4 6.6
NIM 0.1 5.3
KRISS 1 11
MIRS/IJS/F-2,O-2 2 9
EXHM/GCSL-EIM 2.4 11
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Arsenic in bovine liver

NOMINAL VALUE  1 µg/kg to 100 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

LABi Di Uneg,i Upos,i
µg/kg
µg/kg
µg/kg
EXHM/GCSL-EIM -0.94 1.2
LNE -0.8 1.5
NIMT 0.3 2.0
NIM 0.67 1.2
UME 0.7 1.3
INM (CO) 8.8 2.3
VNIIM 14.6 6.3
Participating institutes
CCQM-K145

MEASURAND   Mass fraction of Mercury in bovine liver

NOMINAL VALUE  1 µg/kg to 100 µg/kg

 

Degrees of equivalence represented by Di and its expanded uncertainty Ui at a 95 % level of confidence, both expressed in µg/kg.

LABi Di Uneg,i Upos,i
µg/kg
µg/kg
µg/kg
INM (CO) -3.2 1.7
NIMT -2.0 1.4
MIKES-SYKE -0.79 1.8
HSA -0.25 1.1
NRC -0.2 4.5
RISE -0.2 1.5
MIRS/IJS/F-2,O-2 0.1 1.4
NIM 0.81 1.8
LNE 1.1 1.8
UME 1.1 1.2
VNIIM 2.4 4.3
Participating institutes
CCQM-K145
Comparison
Comparison close
CC comparison
Linked comparison
CCQM-K145
Metrology area, Sub-field Chemistry and Biology, Inorganics
Description Toxic and essential elements in bovine liver powder
Time of measurements 2017
Status Approved for equivalence
Final Reports of the comparisons
Measurand Mass fraction of elements at different concentration levels

P (5 - 50) mg/g ; S (1 - 30) mg/g ; Zn (50 - 500) mg/kg;
Ni, Mn, Mo, Cr (0.1 - 10) mg/g
Sr (50 - 500) µg/kg ; Pb, Co (10 - 300) µg/kg ; Ar, Hg (1 - 100) µg/kg

Transfer device Bovine liver powder samples
Comparison type Key Comparison
Consultative Committee CCQM (Consultative Committee for Amount of Substance)
Conducted by CCQM (Consultative Committee for Amount of Substance)
Comments Results published on 29 July 2020
 
Pilot institute NIM
National Institute of Metrology
China
Contact person J. Wang

+86 10 8425 1244
First Name Last Name
wwww@ww.www +356719836 Institute 1 Institute 1 Khmelnitskiy
Pilot laboratory
NIM

National Institute of Metrology, China, APMP

EXHM/GCSL-EIM

National Laboratory of Chemical Metrology/GCSL - Hellenic Institute of Metrology, Greece, EURAMET

GL

Government Laboratory, Hong Kong, China, APMP

HSA

Health Science Authority, Singapore, APMP

INACAL

National Institute for Quality, Peru, SIM

INM (CO)

Instituto Nacional de Metrología de Colombia, Colombia, SIM

INRAP

Institut National de Recherche et d'Analyse Physico-Chimique, Tunisia, AFRIMETS

INRIM

Istituto Nazionale di Ricerca Metrologica, Italy, EURAMET

KEBS

Kenya Bureau of Standards, Kenya, AFRIMETS

KRISS

Korea Research Institute of Standards and Science, Korea, Republic of, APMP

LATU

Laboratorio Tecnologico del Uruguay, Uruguay, SIM

LGC

Laboratory of the Government Chemist, United Kingdom, EURAMET

LNE

Laboratoire national de métrologie et d'essais, France, EURAMET

MIKES-SYKE

Finnish Environment Institute, Finland, EURAMET

MIRS/IJS/F-2,O-2

MIRS/Jozef Stefan Institute/Low and Medium Energy Physics F2, Environmental Sciences O2, Slovenia, EURAMET

NIMT

National Institute of Metrology (Thailand), Thailand, APMP

NIST

National Institute of Standards and Technology, United States, SIM

NMIA

National Measurement Institute, Australia, Australia, APMP

NMIJ AIST

National Metrology Institute of Japan, Japan, APMP

NMISA

National Metrology Institute of South Africa, South Africa, AFRIMETS

NRC

National Research Council, Canada, SIM

PTB

Physikalisch-Technische Bundesanstalt, Germany, EURAMET

RISE

Research Institutes of Sweden AB, Sweden, EURAMET

UME

TÜBITAK Ulusal Metroloji Enstitüsü, Türkiye, EURAMET

VNIIFTRI

Institute of Physical Technical and Radiotechnical Measurements, Rosstandart, Russian Federation, COOMET

VNIIM

D.I. Mendeleyev Institute for Metrology, Rosstandart, Russian Federation, COOMET

MEASURAND   Mass fraction of Zinc in bovine liver

NOMINAL VALUE  50 mg/kg to 500 mg/kg

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the median of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 456.20 mg/kg      uR = 1.19 mg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

 

MEASURAND    Mass fraction of Nickel in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the median of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 2.022 mg/kg      uR = 0.025 mg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

 

MEASURAND   Mass fraction of Phosphorus in bovine liver

NOMINAL VALUE  5 mg/g to 50 mg/g

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the arithmetic mean of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 11.40 mg/g      uR = 0.10 mg/g

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/g:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

MEASURAND   Mass fraction of Sulfur in bovine liver

NOMINAL VALUE  1 mg/g to 30 mg/g

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the arithmetic mean of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 6.873 mg/g      uR = 0.099 mg/g

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/g:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

MEASURAND   Mass fraction of Manganese in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the median of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 5.745 mg/kg      uR = 0.023 mg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

 

MEASURAND   Mass fraction of Molybdenum in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the median of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 1.548 mg/kg      uR = 0.004 mg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

MEASURAND   Mass fraction of Chromium in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the median of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 4.380 mg/kg      uR = 0.050 mg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in mg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

MEASURAND   Mass fraction of Strontium in bovine liver

NOMINAL VALUE  50 µg/kg to 500 µg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the arithmetic mean of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 321.04 µg/kg      uR = 3.41 µg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in µg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

MEASURAND   Mass fraction of Lead in bovine liver

NOMINAL VALUE  10 µg/kg to 300 µg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the arithmetic mean of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 144.65 µg/kg      uR = 0.59 µg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in µg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

MEASURAND   Mass fraction of Cobalt in bovine liver

NOMINAL VALUE  10 µg/kg to 300 µg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the arithmetic mean of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 126.07 µg/kg      uR = 2.04 µg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in µg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

MEASURAND   Mass fraction of Arsenic in bovine liver

NOMINAL VALUE  1 µg/kg to 100 µg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  are obtained from the arithmetic mean of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 10.57 µg/kg      uR = 0.45 µg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in µg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

MEASURAND   Mass fraction of Mercury in bovine liver

NOMINAL VALUE  1 µg/kg to 100 µg/kg

 

The key comparison reference value xR and its associated standard uncertainty uR  are based on the median of the participants' results excluding outliers results as reported in section 7.4 of the Final Report.

        xR = 15.75 µg/kg      uR = 0.47 µg/kg

The degree of equivalence of laboratory i relative to the key comparison reference value xR is given by a pair of terms, both expressed in µg/kg:

Di = (xi - xR) and its expanded uncertainty Ui at a 95 % level of confidence where Ui = 2 (uR2 + ui2)1/2.

MEASURAND   Mass fraction of Zinc in bovine liver

NOMINAL VALUE  50 mg/kg to 500 mg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  mg/kg mg/kg
INRAP 429.71* 9.48
VNIIM 436* 9
LATU 453 5.6
INACAL 453.1 8.8
GL 453.6 7.7
NMIA 454.1 4.2
NIM (1) 454.5 5.5
KRISS 454.5 6.7
LGC 454.5 3.9
NMISA 454.5 6.1
MIRS/IJS/F-2,O-2 455 14
NIST 456.2 2.0
UME 457 4
HSA 459 7.1
PTB 459.4 1.7
RISE 460.5 3.2
MIKES-SYKE 460.9 11.5
INM (CO) 461 6.5
NRC 462 5
NIMT 462 13.2
NMIJ 462 3
KEBS 474.22* 16.46
INRIM 491.7* 10.0


Note: * reported value is not included in the calculation of the key comparison reference value.

Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND    Mass fraction of Nickel in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  mg/kg mg/kg
VNIIM 0.147* 0.016
NMISA 0.902* 0.038
NIMT 1.65* 0.06
MIRS/IJS/F-2,O-2 1.93 0.11
INM (CO) 1.94 0.06387
GL 1.942 0.092
LNE 1.958 0.075
NIST 1.984 0.020
KRISS 1.993 0.033
INACAL 2.01 0.06
NMIA 2.02 0.05
NIM 2.022 0.023
NMIJ 2.05 0.02
RISE 2.055 0.052
NRC 2.07 0.05
PTB 2.077 0.035
LATU 2.08 0.059
LGC 2.131 0.042
UME 2.15 0.03
HSA 2.18 0.08
KEBS 4.63* 0.94

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Phosphorus in bovine liver

NOMINAL VALUE  5 mg/g to 50 mg/g

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  mg/g mg/g
VNIIM 10.65* 0.24
NMISA 11.203 0.092
NMIJ 11.26 0.07
NIM 11.27 0.12
LATU 11.40 0.12
UME 11.55 0.09
NRC 11.70 0.30


Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Sulfur in bovine liver

NOMINAL VALUE  1 mg/g to 30 mg/g

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  mg/g mg/g
VNIIM 6.22* 0.21
NIM 6.79 0.06
HSA 6.82 0.16
NRC 7.01 0.13

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Manganese in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  mg/kg mg/kg
VNIIM 5.09* 0.18
LNE 5.48 0.27
MIRS/IJS/F-2,O-2 5.57 0.17
EXHM/GCSL-EIM 5.686 0.245
NIMT 5.71 0.13
INRAP 5.74 0.26
NIM 5.75 0.06
KRISS 5.75 0.11
INACAL 5.77 0.10
LATU 5.79 0.12
NMIJ 5.91 0.06
NMISA 6.69* 0.14
INRIM 6.70* 0.18
KEBS 6.71* 0.63

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Molybdenum in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  mg/kg mg/kg
VNIIM 1.34* 0.05
INRAP 1.36* 0.066
LNE 1.41* 0.06
NIMT 1.49 0.02
NMISA 1.532 0.021
KRISS 1.539 0.049
HSA 1.546 0.021
NMIA 1.550 0.015
MIRS/IJS/F-2,O-2 1.55 0.07
INM (CO) 1.551 0.026
NIM 1.559 0.015
KEBS 1.91* 0.11

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Chromium in bovine liver

NOMINAL VALUE  0.1 mg/kg to 10 mg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

 

Labi xi ui
  mg/kg mg/kg
VNIIM 0.345* 0.015
NMISA 1.816* 0.07
NIMT 3.44* 0.11
LNE 4.13 0.15
KRISS 4.184 0.041
NMIA 4.29 0.06
NIM 4.303 0.046
NMIJ 4.37 0.03
LATU 4.38 0.13
RISE 4.39 0.079
HSA 4.44 0.10
UME 4.47 0.09
MIRS/IJS/F-2,O-2 4.55 0.14
INRIM 4.89 0.15
KEBS 5.21* 0.36

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Strontium in bovine liver

NOMINAL VALUE  50 µg/kg to 500 µg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  µg/kg µg/kg
VNIIM 319 9
NIM 321.0 4.7
NIMT 321 9
LATU 321.2 4.3
NRC 323 9

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Lead in bovine liver

NOMINAL VALUE  10 µg/kg to 300 µg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  µg/kg µg/kg
VNIIM 141.8 4
NIMT 142 3
LATU 142.2 3.0
INM (CO) 143.4 4.3
LNE 143.8 2.5
LGC 143.8 1.2
MIKES-SYKE 144.0 5.0
NIM 145.30 1.15
KRISS 145.6 2.8
UME 145.6 1.3
HSA 145.8 2.6
NRC 147 5
PTB 147.8 2.6
NMISA 150.2 2.3
KEBS 159.49* 26.09

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Cobalt in bovine liver

NOMINAL VALUE  10 µg/kg to 300 µg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  µg/kg µg/kg
VNIIM 98.6* 3.2
NIMT 121 5.6
LATU 125.7 2.6
NIM 126.2 1.7
KRISS 127 5
MIRS/IJS/F-2,O-2 128 4
EXHM/GCSL-EIM 128.5 4.9

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Arsenic in bovine liver

NOMINAL VALUE  1 µg/kg to 100 µg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  µg/kg µg/kg
EXHM/GCSL-EIM 9.63 0.44
LNE 9.8 0.6
NIMT 10.9 0.91
NIM 11.24 0.42
UME 11.3 0.5
INM (CO) 19.4* 1.1
VNIIM 25.2* 3.1

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report

MEASURAND   Mass fraction of Mercury in bovine liver

NOMINAL VALUE  1 µg/kg to 100 µg/kg

 

xi    measurement value reported by participant laboratory i, Lab i

ui   combined standard uncertainty of xi

Labi xi ui
  µg/kg µg/kg
INM (CO) 12.6* 0.69
NIMT 13.8 0.52
MIKES-SYKE 14.96 0.75
HSA 15.50 0.33
NRC 15.6 2.2
RISE 15.6 0.62
MIRS/IJS/F-2,O-2 15.9 0.5
NIM 16.56 0.78
LNE 16.9 0.8
UME 16.9 0.4
VNIIM 18.2 2.1

Note: * reported value is not included in the calculation of the key comparison reference value.
Note: VNIIM is referred to as UNIIM in the Final report